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A consolidated method for the analysis of VOCs in soil by HS 4 µL aliquot of the appropriate standard solution to a 20 mL headspace vial (P/N 20-CV) and sealed with magnetic caps (P/N 20-MCBC). This produced standards in the range 10–500 µg/kg (ppb) with internal standards at 50 µg/kg.

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20 mL headspace vial (P/N 20-CV) and sealed with magnetic caps (P/N 20-MCBC). This produced standards in the range 10–500 µg/kg (ppb) with internal standards at 50 µg/kg. Samples were prepared by adding 2 g of locally sourced soil to a 20 mL headspace vial and adding 10 mL of matrix modifying solution and 4 µL of internal standard. The vials