Stock Solution. Label vial as “25 ppm ETC Standard”. 5. Using a micropipettor, add to the third vial, 50 µL of the 1 mg/mL ETC Stock Solution. Label vial as “50 ppm ETC Standard”. 6. Gently evaporate the n-hexane from the standard vials using a low N2 8.
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Static headspace GC (SH-GC) is a commonly used technique in the analysis of these OVIs. This technique concentrates volatile analytes, and allows for their analysis free from sample matrix. Samples to be analyzed by SH-GC must be dissolved in a suitable solvent; and in addition to being able to dissolve the sample, the solvent chosen must allow for sufficient sensitivity of the analytes of
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Methanol, analytical grade It must be checked that no interfering amine and nitrosamine compounds are present. Helium, 5.0 (99.999%) Oxygen, 5.0 (99.999%) 1.3 Solutions Dichloromethane/methanol mixture: In a 100 mL volumetric flask 25 mL methanol is N
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Serum Vials & Accessories Overview VIALS Clear 2.5ml 13mm 4ml 13mm 7.5ml 20mm 10ml 13mm 10ml 20mm 13ml 13mm 13ml 20mm 20ml 50ml 100ml 20mm 100ml 32mm CatNo CTSC-2V-13T CTSC-4V-13T CTSC-7V-13T CTSC-10V-13T CTSC-10V-20 CTSC
Vial, Closure and Septa Selection Guide Use this as a guide to selecting the products you need. For technical assistance, contact Supelco Technical Service at (800) 359-3041 or e-mail us at techservice@sial.com. Screw Top Vials. These standard and large
2 1. SCOPE This capillary gas chromatography (GC) method provides for the determination of dihydrosafrole (DHS) as relevant impurity in Piperonyl butoxide (PBO) technical grade active ingredient. O O IUPAC name : 5-propyl-1,3-benzodioxole CAS n 94-58-6
Derivatization of external calibration standards was achieved by adding 0, 20, 100 and 200 µL of the 100 ng g-1 stock solution to 5 mL acetate/acetic acid buffer (0.1 M) at pH 3.9, adding 2 mL isooctane and 1 mL 1% Na BPr4 (in 18.2 MΩ water) and agitating the
20mm (9) 24mm (8) Vial Color Amber (2) Clear (7) Vial Material Borosilicate Glass (4) USP Type 1 Borosilicate Glass (5) Cap Color Aluminum (1) Blue Aluminum Magnetic (1) Working Volume in
A stock standard solution of 1000 µg/mL of phthalate esters listed in Table 1 was prepared in hexane / acetone (8:2 The solution mixture was shaken vigorously. An aliquot of organic layer was transferred to the GC vial. A high injector temperature (320 C the ...