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funnel, collecting into a 500 mL round bottom flask. f) Concentrate combined extracts to 1-2 mL using a rotary evaporator or equivalent. g) Quantitatively transfer extract to a 4-7mL glass vial using ~ 1 mL portions of MTBE or methanol for rinsing.
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NiNPs (100mg) were then dispersed in 10ml of n-hexane in a 100ml one-neck round-bottom flask. PVP 29K (700mg) was dissolved in 6ml of chloroform and added to the flask. The flask was stoppered, placed under an Ar atmosphere, then stirred and heated at